Guidance on lithiation/metallation reaction

Guidance on lithiation/metallation reaction

Hello great chemists,

I need to run this synthesis (photo attached) at lab scale and I'm new to lithium metal/organolithium chemistry, so I want to understand the protocol properly before I do it.

Can anyone walk me through how to actually execute this step by step, what to watch out for since lithiation feels dangerous to me, and where to source 30% Li dispersion in mineral oil in the US? Any practical tips appreciated. Thank you very much in advance for your time!

https://preview.redd.it/dc4k2arhx9gh1.png?width=1922&format=png&auto=webp&s=173f818ffa64174b79915179b73e8beedaeee349

submitted by /u/Euphoric_Attitude979
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